PYROXSULAM

  • CasNo:422556-08-9
  • Purity:
  • Molecular Formula:C14H13 F3 N6 O5 S
  • Molecular Weight:434.356
  • Melting Point:  
  • Apply:
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Factory Supply Industrial Grade PYROXSULAM 422556-08-9 with Best Price

  • Molecular Formula:C14H13 F3 N6 O5 S
  • Molecular Weight:434.356
  • Refractive Index:1.633 
  • Boiling Point:°Cat760mmHg 
  • PKA:1.92±0.30(Predicted) 
  • Flash Point:°C 
  • PSA:138.21000 
  • Density:1.68g/cm3 
  • LogP:2.51850 

PYROXSULAM(Cas 422556-08-9) Usage

InChI:InChI=1/C14H13F3N6O5S/c1-26-8-6-9(27-2)23-13(19-8)20-12(21-23)22-29(24,25)10-7(14(15,16)17)4-5-18-11(10)28-3/h4-6H,1-3H3,(H,21,22)

422556-08-9 Relevant articles

CRYSTALLINE FORMS OF N-(5,7-DIMETHOXY-[1,2,4]TRIAZOLO[1,5-A]PYRIMIDIN-2-YL)-2-METHOXY-4-(TRIFLUOROMETHYL)PYRIDINE-3-SULFONAMIDE

-

Page/Page column 16-19, (2020/10/09)

The present invention relates to novel c...

A dingding sulphur grass amine preparation method (by machine translation)

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Paragraph 0015-0016; 017, (2019/01/06)

The invention provides a method for prep...

Application of the tisler triazolopyrimidine cyclization to the synthesis of a crop protection agent and an intermediate

Bell, Bruce M.,Fanwick, Phillip E.,Graupner, Paul R.,Roth, Gary A.

, p. 1167 - 1171 (2012/12/23)

A new synthetic route to the Dow AgroSci...

Process for the preparation of N-([1,2,4]triazolopyrimidin-2-yl)aryl sulfonamides

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Page/Page column 5, (2008/06/13)

The N-arylsulfilimine-catalyzed coupling...

422556-08-9 Process route

5,7-dimethoxy-[1,2,4]-triazolo-[1,5-a]-pyrimidin-2-amine
13223-43-3

5,7-dimethoxy-[1,2,4]-triazolo-[1,5-a]-pyrimidin-2-amine

2-methoxy-4-(trifluoromethyl)-pyridine-3-sulfonyl chloride
219715-41-0

2-methoxy-4-(trifluoromethyl)-pyridine-3-sulfonyl chloride

pyroxsulam
422556-08-9

pyroxsulam

Conditions
Conditions Yield
5,7-dimethoxy-[1,2,4]-triazolo-[1,5-a]-pyrimidin-2-amine; 2-methoxy-4-(trifluoromethyl)-pyridine-3-sulfonyl chloride; With dmap; In dichloromethane; for 0.5h;
With triethylamine; In dichloromethane; at 20 - 35 ℃; for 3h; Temperature;
94%
With 3,5-Lutidine; dimethyl sulfoxide; In acetonitrile; at 20 ℃; for 12h; Product distribution / selectivity;
82%
With 3,5-Lutidine; N-(5,7-dimethoxy[1,2,4]triazolo[1,5-a]pyrimidin-2-yl)-S,S-dimethyl-sulfilimine hydrochloride salt; In acetonitrile; at 20 ℃; for 22h; Product distribution / selectivity;
78%
With 3,5-Lutidine; In dimethyl sulfoxide; acetonitrile; at 25 ℃; for 16h; Reagent/catalyst; Inert atmosphere;
C<sub>15</sub>H<sub>13</sub>F<sub>3</sub>N<sub>6</sub>O<sub>7</sub>S

C15H13F3N6O7S

pyroxsulam
422556-08-9

pyroxsulam

Conditions
Conditions Yield
In toluene; acetonitrile; at 20 - 35 ℃; Inert atmosphere;
83%

422556-08-9 Upstream products

  • 13223-43-3
    13223-43-3

    5,7-dimethoxy-[1,2,4]-triazolo-[1,5-a]-pyrimidin-2-amine

  • 219715-41-0
    219715-41-0

    2-methoxy-4-(trifluoromethyl)-pyridine-3-sulfonyl chloride

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